rpar

A list of some of the available 500wb MHz expts

rpar - if you type 'rpar' and then enter you should see a list of all expts. focus on the lower case for now as these are experiments i've built for this NMR.

macro: - for 'macro' below these are known as "macros". just type it into the command line of topspin and the experiment will load. note macros are filled with commands that you normally just type into the command line.

90_times -- measured 90s for the 5mm TXI probe recently.

1D:

macro: h1.txi -- 1D Proton -- pulprog
macro: h1_es.txi -- 1D Proton with excitation sculpting water suppression -- pulprog
macro: selnoe.txi -- 1D NOE Proton -- pulprog
macro: selroe.txi -- 1D ROE Proton; used for MW of 700-1100 Da where NOEs don't show well. -- pulprog
- cnst21 is the peak selected in ppm
- using a 200ms mix time at 10kHz RF Field
macro: c13.txi -- 1D 13C -- pulprog
macro: f19.txi -- 1D 19F; need to wobb to 19F tuning using 1H tuners. -- pulprog
- wobb using the "yellow" tuners
- at zg/rga type in password "topspin" to make error go away
- optional: set o1p near your peak if far away. This is the center of spectrum in ppm
macro: std1d.txi -- STD Saturation Transfer Difference for ligand binding. -- ref1 -- macro_to_set_expt -- pulprog

2D:

macro: kinetic_2d -- Series of 1D experiments for Kinetics (pseudo 2D file storage). See macro for defining delays etc. -- pulprog
macro: h1_t2.txi -- Proton T2 measurement (pseudo 2D file storage). See macro for defining delays etc.
- pulprog -- pulse program
- mk_t2.pl -- perl script to make delays and loop files
- t2_list -- t2 looping file in VC directory
- t2_list.txt -- t2 delay values
macro: noesy.txi -- 2D NOESY without water suppression. -- pulprog
macro: cosy.txi -- 3 Pulse DQF COSY with gradient selection (organic compounds). Note it's magnitude mode. -- pulprog
macro: clipcosy.txi -- Clip COSY - Clean in-phase COSY. Only see doublets (use this). -- ref1 -- pulprog
macro: c_hsqc.txi -- H/C HSQC experiment. -- pulprog
macro: c_h2bc.txi -- H/C 2-bond correlation experiment. -- pulprog -- ref
macro: c_hmbc.txi -- H/C HMBC experiment. -- pulprog
macro: qhsqc.txi - Quantitative H/C 2D HSQC -- ref1 -- hsqc_info
macro: dosy.txi -- DOSY without water suppression. -- pulprog

2D in Water:

macro: cosy_es.txi -- COSY with water suppression. -- pulprog
macro: noesy_es.txi -- NOESY with water suppression. -- pulprog
macro: roesy_es.txi -- ROESY with water suppression. Use for case where we can't see NOESY due to molecular size. -- pulprog
macro: tocsy_es.txi -- TOCSY with water suppression. -- pulprog
macro: dosy_es.txi -- DOSY with 3-9-19 water suppression. -- pulprog
macro: ipcosy.txi -- In-Phase COSY with water suppression. 3J from HN/HA correlations. -- ref1 -- pulprog