;C.90 ;;version: 1.0/ TS3.2 /2013/07/12 ;written for BioToolkit: VEDA July 2013 ;double-checked: VEDA SEWE July 2013 ;direct excitation and acquisition on C ;Avance II / III version ;parameters: ;p1 : C 90 at pl1 ;pl1 : C pulse power ;d1 : recycle delay ;ns : 4 (full:4) ;cnst31 : =MAS spin rate (or =1e6 for static) ;l1 : # of rotor cycles (or tau in us) ;$COMMENT= single pulse excitation, acquisition without decoupling ;$CLASS=BioSolids ;$DIM=1D ;$TYPE=direct excitation ;$SUBTYPE=Setup prosol relations= #include ; defines which channel corresponds to which nucleus #include ; definition of external trigger output ;"acqt0=-p1*2/3.1416" "acqt0=0" ;########################## ;$EXTERN ;# Python insertion point # ;########################## Prepare, ze ;###################################################### ;# Protections: Pre-Check # ;###################################################### "p2=p1*2" "d6=((1s*l1)/cnst31)-(p1/2)-(p2/2)" ;###################################################### ;# Start of Active Pulse Program # ;###################################################### Start, 30m d1 do:H trigg 1u trigpe4 ;MAS trigger ; 1u fq=0.0:C ;set 13C on resonance 1u cw:H pl13:H ;pl12 is used here with tppm, spinal, pl13 with cwlg, cwlgs (p1 pl1 ph1):C d6 (p2 pl1 ph2):C d6 ;####################################################### ;# Acquisition # ;####################################################### 0.1u do:H 1u cpds2:H pl12:H ;pl12 is used here with tppm, spinal, pl13 with cwlg, cwlgs go=Start ph31 1m do:H 30m mc #0 to Start F0(zd) HaltAcqu, 1m Exit, exit ;##################################### ;# Phase Cycle # ;##################################### ph1= 0 2 1 3 ; C hard pulse ph2= 1 3 0 2 ; C hard pulse ph31=0 2 1 3 ; receiver ;####################################################### ;$Id: C.90,v 1.1.2.2 2013/08/29 14:03:53 ber Exp $