#rpar hNCaCx3D all rpar ncacx3d.1p3 all pulprog ncacx3d_rfdr.dm ############################## ## H SETTINGS # ############################### p3 2.5u #H90 plw2 8.2 #H90 power spw42 0.28 #H cp power (1/3)*wr spnam42 Tang_cp_80p #H cp shape p25 1.25m #CP pulse length cpdprg2 spinal64_v2 #H dec during acqu pcpd2 50u #H tppm15 length plw22 0.08 #H spinal64 power; use spinal64 not tppm plw33 0.0 #H tppm15 power during cn cp cpdprg3 cwlgs_13 #H dec during rfdr cnst20 100000 #H LG rf field plw13 0 #H LG power to get 100khz plw33 0 #H cw during cp ############################## # N SETTINGS # ############################## spnam43 square.1000 #N-H CP shape spw43 8.2 #N-H CP power; match (2/3)*wr p16 8.5m #N-C cp time plw5 10.0 #N-C CP power; match 38khz field p21 4.4 #N 90 composite t2 p22 8.8 #N 180 composite t2 plw21 20 #N 90 power level watts ############################## # C SETTINGS # ############################## spw50 0.78 #N-C cp power 12khz spnam50 TangCP_80p_down #N-C cp shape p1 2.6u #C 90 hard time p2 5.2u #C 180 hard time plw1 35.0 #C 180 power p12 6.67u #C 180 for rfdr plw11 24.69 #C power for 180 rfdr 0.333*taur l1 160 #l1=16*n; 160->3.2ms at vr=50k zgoptns -Dfprfdr # use for above 20khz vr ############################## cnst22 172 #CO or CA offset 170ppm/45ppm cnst26 172 #t2 (ca/co) center #cnst10 100 #C center for detection set internally by o1p cnst23 98 #RFDR offset 45ppm/100ppm cnst31 50000 #spin rate o3p 125 #15N center ppm o2p 4.3 #1H center ppm o1p 100 #13C center ppm 1 sw 50 #N sw for indirect PPM 1 td 32 #3m 2 sw 40 #C sw ppm; high vr 2 td 64 #4m #3 sw 200 #C sw ppm; high vr 3 swh 50000 #C sw Hz; high vr 3 td 1k #35m 1 FnMode States-TPPI 1 MC2 States-TPPI 2 FnMode States-TPPI 2 MC2 States-TPPI ns 80 rg 2050 ds 16 d1 1.5s ############################## ############################## ##############################