rpar hCONCaCx3D.dm all pulprog hCaNCOCX3D.tcp.dm ZGOPTNS -DnoMix ############################## # H SETTINGS # ############################## p3 2.5u #H90 plw2 8.2 #H90 power spw40 1.46 #H cp power 38khz spnam40 Tang_cp_80p #H cp shape p15 0.50m #CP pulse length cpdprg2 spinal64_v2 #H dec during acqu pcpd2 50u #H tppm15 length plw22 0.08 #H spinal64 power; use spinal64 not tppm plw33 0.0 #H tppm15 power during cn cp plw34 0.0 #H tppm15 power during cn cp plw12 0.0 #H turn off decoupling during t1/t2 ############################## # N SETTINGS # ############################## #N SETTINGS 2nd CP p16 8.5m #C-N cp time spnam5 TangCP_80p_down #C-N CP shape spw5 2.12 #C-N CP power; match wr/3 #N SETTINGS 3rd CP p17 4m #N-C cp time spnam6 CW_1000_100pcnt #N-C CP shape spw6 9.65 #N-C CP power; match 38khz field plw21 15.5 #N : 90/180 comp power p21 5.0u #N : 90 composite during t2 pl21 p22 10.0u #N : 180 composite during t2 pl21 ############################## # C SETTINGS # ############################## #C SETTINGS 1st CP spw41 0.70 #C CP HC 12kHz spnam41 CW_1000_100pcnt #C CP HC shape #C SETTINGS 2nd CP spw50 4.70 #C-N cp power 2wr/3 spnam50 CW_1000_100pcnt #C-N cp shape #C SETTINGS 3rd CP spw51 0.78 #N-C cp power 12khz spnam51 TangCP_80p_down #N-C cp shape p1 3.33u #C 90 hard time p2 6.66u #C 180 hard time plw1 24.69 #C 180 power and rfdr ############################## 1 sw 40 #C sw for indirect 1 td 64 #5m 2 sw 50 #N sw ppm; high vr for indirect 2 td 32 #5m 3 sw 200 #C sw for direct 3 td 1k #25m o3p 125 #15N center ppm o2p 4.3 #1H center ppm o1p 100 #13C center ppm; composites during 15n evol cnst22 178 #C center for co transfer; t1 cnst21 55 #C center for ca transfer; t3 #cnst10 100 #is o1p C center for detection in t3 100 and fprfdr center cnst31 50000 #spin rate cnst29 0 #td1 cnst duty cycle cnst30 0 #td2 cnst duty cycle #l1 160 #l1=16*n; 160->3.2ms at vr=50k #zgoptns -Dfprfdr # use for above 20khz vr 1 FnMode States-TPPI 1 MC2 States-TPPI 2 FnMode States-TPPI 2 MC2 States-TPPI ns 96 rg 2050 ds 16 d1 1.5s ############################## ############################## ##############################