rpar cpmas_20k.1p9 all pulprog pithirds2_notrig.dm p21 2.7u #H90 plw2 13.4 #H90 power spw0 22.2 #H cp power spnam0 tacn50 #H cp shape p15 3m #CP pulse length cpdprg2 tppm15 #H dec during acqu pcpd2 5.2u #H tppm15 length plw12 13.4 #H tppm15 power cpdprg3 cwlgs_13 #H dec during rfdr cnst20 100000 #H LG rf field plw23 15.63 #H LG power to get 100khz #note cnst22 cnst23 and p5 calcd in lgcalc.incl plw1 8.1 #C CP power p1 4.5u #C 90 hard time plw11 43.0 #C 90 hard power #p2 16.7u #C 180 for rfdr 1/(3*vr) plw17 12.3 #C power for 180 rfdr #cnst10 100 #C detect frequency ppm #cnst11 15.3 #C RFDR frequency ppm cnst31 20000 #spin rate l1 4 #k1 repeats a,b and c l2 32 #k2 elements for CT evolution not dipolar recoupling l3 0 #k3 elements for recoupling l4 4 #k4 rotor cycles each a b c #zgoptns -Dfprfdr #use for above 20khz vr 1 swh 20000 #swh for direct 1 td 1700 #PSL params cnst35 1 #spin lock detection enhancement acq 0=no plw16 34.8 #C 180 PSL power p2 10u #C 180 PSL d12 45u #C PSL ring down tau2 l22 40 #C PSL number of echoes to acquire l30 20 #C PSL rotor cycles per echo #adjust l30 to get tau1 = 450u o2p 4.3 #1H center ppm #o1p 170.2 #13C center ppm o1p 54.1 #13C center ppm ns 3600 rg 2050 ds 64 d1 3s