rpar hCONCaCx3D all #vr 9khz #F3 CA dir; F2 N indir; F1 CO indir pulprog hCaNCOCX3D.tcp.dm ############################### # H SETTINGS # ############################### p3 3.0u #H90 plw2 13.4 #H90 power spnam40 ramp10090.100 #H cp shape spw40 9.7 #H cp power; rf=7.5wr p15 2.0m #CP pulse length cpdprg2 tppm15 #H dec during acqu pcpd2 5.6u #H tppm15 length plw12 13.4 #H tppm15 power cnst20 100000 #H LG rf field plw33 20.6 #H LG power to get 100khz ############################### # N SETTINGS 2nd CP # ############################### p16 6.0m #C-N cp time; popt spnam5 ramp10090.100 #CP shape spw5 61.2 #C-N CP power; match rf=3.5wr; popt ############################### # N SETTINGS 3rd CP # ############################### p17 6.0m #N-C cp time; popt spnam6 square.100 #N-C CP shape spw6 51.25 #N-C CP power; match 3.5wr; popt plw21 100 #N : 90/180 comp power p21 5.8u #N : 90 composite during t2 pl21 p22 11.6u #N : 180 composite during t2 pl21 ############################### # C SETTINGS 1st CP H->C # ############################### spw41 48.9 #C CP HC 6.5wr; >50khz spnam41 square.100 #C CP HC shape ############################### # C SETTINGS 2nd CP Co->N # ############################### spw50 7.2 #C-N cp power 2.5wr spnam50 square.100 #C-N cp shape ############################### # C SETTINGS 3rd CP N->Ca # ############################### spw51 8.0 #N-C cp power 2.5wr spnam51 ramp10090.100 #N-C cp shape p1 4.50u #C 90 hard time p2 9.00u #C 180 hard time plw1 44.0 #C 180 power and rfdr ############################### 1 swh 3000 #CO swh for indirect wr/3 1 td 48 #9m 2 swh 2250 #N swh for indirect wr/4 or wr/3 2 td 40 #8m 3 swh 27000 #Ca swh for direct 3wr 3 td 768 #13m o2p 3.8 #1H center ppm o1p 55 #C center ppm o3p 120 #15N center ppm 1 o1p 55 #Co center t1; gets overwritten by 3 o1p 2 o1p 120 #N center t2 3 o1p 55 #Ca center t3 detect ca cnst10 100 #C composites center during N-t2 center cnst22 175 #C center for co transfer; t1 indir center cnst21 55 #C center for ca transfer; t3 dir center cnst31 9000 #spin rate cnst29 0 #td1 cnst duty cycle cnst30 0 #td2 cnst duty cycle 1 FnMode States-TPPI 1 MC2 States-TPPI 2 FnMode States-TPPI 2 MC2 States-TPPI ns 128 rg 256 ds 32 d1 1.0s ############################### ############################### ###############################